URN | etd-0704116-104434 | Statistics | This thesis had been viewed 331 times. Download 4 times. |
Author | Ke-Lun Wang | ||
Author's Email Address | je2499@yahoo.com.tw | ||
Department | Institute Of Mechanical Engineering | ||
Year | 2015 | Semester | 2 |
Degree | Master | Type of Document | Master's Thesis |
Language | zh-TW.Big5 Chinese | Page Count | 110 |
Title | Effect of added nano AlN on the microstructure and mechanical properties of the vitrified bond diamond tools | ||
Keyword | |||
Abstract | ABSTRACT The goals of this study were to investigate the influence of added nano-AlN powders on the microstructure and mechanical properties of the vitrified bond diamond tools. The sintering temperature of the specimens was 660C and isothermal holding for 90 min. All of the sintered specimens were examined using an X-ray diffraction analyzer, a Raman spectrometer analyzer, a scanning electron microscope, a hardness test and a grinding ratio test. DSC analysis showed that the glass transition temperature (Tg) for the borosilicate glass powder used in this study was approximately 716C. XRD patterns showed no phase other than diamond and AlN were observed. A sharp peak at 1330.2 cm-1 can be observed which belongs to the crystalline diamond C-C bond D-band signal. Adding of 10 vol.% to 20 vol.% nano-AlN powders in the vitrified bond diamond tools protect the diamond crystal during sintering process. SEM image shows that specimen added with 10 vol.% nano-AlN powders had excellent coverage and wetting between the diamond grits and vitrified bond. The brittle fracture of cleavage was observed on the vitrified bond surface after grinding test, and allowing the diamond grit to fall off after abrasion. Therefore, the highest grinding ratio of the diamond tool and the best surface roughness of work piece were achieved. Keywords: Nano Aluminum nitride, Sintering parameters, Vitrified bond diamond tools, Microstructure, Mechanical properties. |
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Advisor Committee | |||
Files | indicate in-campus access immediately and off-campus access at 2 years | ||
Date of Defense | 2016-05-02 | Date of Submission | 2016-07-05 |